rp hplc Search Results


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MACHEREY NAGEL ec 4 3 nucleoshell rp 18 plus guard column
Ec 4 3 Nucleoshell Rp 18 Plus Guard Column, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 94/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL rp hplc analytical runs
Rp Hplc Analytical Runs, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 94/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL nucleodur sphinx rp column
Nucleodur Sphinx Rp Column, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL preparative hplc method b
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Preparative Hplc Method B, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Average 90 stars, based on 1 article reviews
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MACHEREY NAGEL rp hplc
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Rp Hplc, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 91/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL nucleoshell rp 18 plus column
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleoshell Rp 18 Plus Column, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Average 93 stars, based on 1 article reviews
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MACHEREY NAGEL nucleoshell rp 18 column
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleoshell Rp 18 Column, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Average 93 stars, based on 1 article reviews
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MACHEREY NAGEL nucleocel delta rp s
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleocel Delta Rp S, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL ec hplc guard column nucleodur
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Ec Hplc Guard Column Nucleodur, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 91/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL nucleoshell bluebird rp 18
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleoshell Bluebird Rp 18, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 92/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL nucleodur 100 5 nh2 rp column
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleodur 100 5 Nh2 Rp Column, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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MACHEREY NAGEL nucleoshell rp18 2 7 lm
Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : <t>preparative</t> <t>HPLC</t> (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).
Nucleoshell Rp18 2 7 Lm, supplied by MACHEREY NAGEL, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Image Search Results


Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : preparative HPLC (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).

Journal: Molecules

Article Title: Antileishmanial and Cytotoxic Compounds from Valeriana wallichii and Identification of a Novel Nepetolactone Derivative

doi: 10.3390/molecules20045740

Figure Lengend Snippet: Overview of the bioassay-guided fractionation of V. wallichii extract. Method A : preparative HPLC (250 mm × 10 mm, 5 µm, Nucleosil 100-5); H 2 O (a): MeOH (b), gradient: 70% b (0 min), 75% b (7 min), 100% b (25 min), 70% b (30 min); flow rate: 3.3 mL/min. Method B : preparative HPLC (125 mm × 10 mm, 5 µm, Nucleodur Sphinx RP); H 2 O (a): CH 3 CN (b), gradient: 10% b (0–2 min), 30% b (2–15 min), 65% b (15–22 min), 10% b (22–24 min); flow rate: 4.4 mL/min. Method C : flash chromatography (silica gel; MeOH/CHCl 3 , 4.8:0.2, v/v ). Method D : column chromatography (silica gel; MeOH/CHCl 3 , 4.8:02, v/v ).

Article Snippet: A portion of 600 mg of fraction F1 was further fractionated by preparative HPLC method B (125 mm × 10 mm, 5 μm, Macherey-Nagel Nucleodur Sphinx RP; A) H 2 O, B) CH 3 CN, gradient: 10% B (0–2 min), 30% B (2–15 min), 65% B (15–22 min), 10% B (22–24 min); flow rate: 4.4 mL/min) resulting in 9 fractions (F1-1 to F1-9).

Techniques: Bioassay, Fractionation, Chromatography, Column Chromatography